The crystallinity of the catalysts was measured by powder X-ray diffraction (XRD) on a Bruker AXS D8 Discover diffractometer with monochromatic Cu–Kα radiation (1.5406 Å) from 5 to 50° 2θ.
According to the method already reported (31), the crystal structure was determined using an X-ray diffractometer (Bruker AXS Ltd., Leipzig, Germany), and the relative crystallinity was calculated ...
The spectra were recorded on a BRUKER ADVANCE DPX 300 and 400. Powder wide angle XRD patterns were obtained on a BRUKER AXS D5005 X-ray diffractometer, using a CuKα radiation (λ = 1.54184 Å) as X-ray ...
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